Re: Freeze Dryer, Vacuum Pump and Oil filter Problems!

From: Steve Turner (spam_at_spam.net)
Date: 07/29/04

  • Next message: Muhammar: "Re: Freeze Dryer, Vacuum Pump and Oil filter Problems!"
    Date: Thu, 29 Jul 2004 02:02:39 GMT
    
    

    On 28 Jul 2004 11:25:13 -0700, princzma@mcmaster.ca (Marta) wrote:

    >Second, I have been going through oil mist filters rather quickly --
    >any ideas why? I've read this might be due to improper maintenance on
    >the pump/oil system, eg. moisture in the oil. How often (in hours of
    >usage) should I perform an oil change in the pump? Unfortunately the
    >system was not purchased with an oil drain kit... Also, I've heard
    >about running the pump with the gas ballast open -- what does this
    >mean? And is this necessary if I have an oil recirculation filter
    >(provided it is working properly?)

    I am not familiar with your specific model so I can't help directly
    with most of your questions. However, I do have some general comments
    regarding care of laboratory-sized lyophilizers:

    Most belt-driven vacuum pumps have a "ballast" valve which can be
    adjusted to bleed air into the pump. Lyophilizer manuals always
    recommend operating the pump with the ballast open, because the air
    bleed helps to purge the pump oil of water and/or other volatiles.
    These volatiles will reduce the highest achievable vacuum and can also
    cause internal corrosion of the pump. The problem with running with
    the ballast open is that it causes oil mist ... as you observed.

    In fact, we have found use of the ballast to be unacceptable for this
    reason, and we have always operated with the ballast closed. With
    reasonable care this does no harm. Reasonable care includes: 1) water
    ONLY on the lyophilizer; anyone putting volatile organics on the
    system will be strung up by the testicles; 2) the pump oil should be
    changed frequently, say after every ~2L of water has collected, or
    immediately if the oil appears cloudy; 3) the vac pump should never be
    on unless the condenser is as cold as it will get.

    Steve Turner


  • Next message: Muhammar: "Re: Freeze Dryer, Vacuum Pump and Oil filter Problems!"

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