Gravimetric Analysis.
- From: rain.on.moon@xxxxxxxxx
- Date: 1 Jul 2005 01:02:21 -0700
Dear All,
I am in the middle of nowhere. I have had a reaction to synthesize
tributyl phosphate. The reactants were phosphorus oxychloride,pyridine
and n-butanol. Now that the reaction is complete. I want to get the
organic layer separated in the separating funnel analysed. I want to
know how much quantities of tributyl phosphate, dibutyl phosphate,
monobutyl phosphate, water and butanol are present in the separated
organic layer. I have searched for all th available methods of analysis
but they are qualitative. I want to know if there is any method that
gives us the percentage of the above mentioned entities. Any sort of
help will be appreciated.
Regards.
.
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