Re: Amateur FTIR



"Douglas Taylor" <dj.taylor@xxxxxxxxxxxxx> writes:

> "Sam Goldwasser" <sam@xxxxxxxxxxxxxxxxxx> wrote in message
> news:6wk6fhdwjv.fsf@xxxxxxxxxxxxxxxxxxxxx
> > "Douglas Taylor" <dj.taylor@xxxxxxxxxxxxx> writes:
> >
> >> Is it possible to build your own FTIR?
> >>
> >> I don't mean from scratch, I mean is it possible to build one out of
> >> 'parts'.
> >
> > Sure, why not? :)
> >
> >> I ask because I just bought the electronics and beamsplitter/moving
> >> mirror
> >> assembly from a Nicolet Spectrometer. The moving mirror is a 'porch
> >> swing'
> >> type so I don't need air for an air bearing, the KBr beamsplitter looks
> >> in
> >> excellent shape. It would be neat to get this working in a stand-alone
> >> mode.
> >
> > You may be better off ignoring the electronics except maybe the detector
> > front-end and doing your own unless documentation is available.
>
> I have given this some thought.... The electronic functions that are needed
> are:
>
> 1. Amp to drive the mirror motor - sort of a saw tooth drive signal
> (audio freq bandwidth)
> 2. Laser signal phase lock loop - if the mirror moves at a constant
> speed the laser interference signal will be a sine wave in the audio
> spectrum, I think you couple this to the mirror drive to keep the mirror
> speed constant.

So these together form a constant reference frequency drive.

> 3. A/D trigger signal - you use the laser reference zero crossings to
> trigger the A/D

Is that a high enough sampling rate? I guess if it's IR, then the fringe
signal for the unknown spectrum will be a lower frequency but you still
need to obey Mr. Nyquist.

> 4. Start & End of scan - you need to know where the mirror is, either at
> the start of the scan or end and either direct the mirror drive circuit to
> tell the mirror motor to go forward or backward.
> 5. Digital interface - connect the A/D to a computer, monitor other
> signals.
>
> Sounds like a lot of basic electrical circuit stuff, nothing exotic. Maybe
> it is possible to build.

> >> I still need an laser and detector (working on it), but the real question
> >> is can I operate the electronics independently?

> > You mean a laser for the reference?

> Yes, an ordinary HeNe laser is what is used. The beamsplitter I have
> has a small circular area in the middle which is where the laser reference
> beam is directed. I comes out the other side of the interferometer into a
> small detector.

So it sounds like you have an interesting project if you're in it for
the challenge. Even if you don't do the full FTIR, you could build a
nice accurate wavemeter with what you have.

--- sam | Sci.Electronics.Repair FAQ: http://www.repairfaq.org/
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